Hydrochloric Acid → HCID 10036204, compound

HRID 2239205Notes

Reaction equation

HRID 2239205 reaction equation
[CH2:1]=[O:2].[C:3]12([CH2:13]O)[CH2:12][CH:7]3[CH2:8][CH:9]([CH2:11][CH:5]([CH2:6]3)[CH2:4]1)[CH2:10]2.[ClH:15]>>[Cl:15][CH2:1][O:2][CH2:13][C:3]12[CH2:12][CH:7]3[CH2:6][CH:5]([CH2:11][CH:9]([CH2:8]3)[CH2:10]1)[CH2:4]2

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 712FormaldehydeHCID 64556Tricyclo(3.3.1.1'3,7)dec-1-ylmethanol2×

Product 1

HCID 10036204HCID 10036204, compound

Procedure

Paraformaldehyde was added to adamantane-1-methanol, and a hydrogen chloride gas was injected at 2.5 equivalent amounts per this adamantane-1-methanol. Then, the reaction was conducted at a temperature of 50° C. for 12 hours. After the completion of the reaction, the product was distillated under reduced pressure so as to obtain 1-adamantylmethyl chloromethyl ether (compound 3) represented by the following chemical formula (60).

Workup

  1. customAfter the completion of the reaction

Sources & evidence

ORD record
ord-2bb08e7a03e845669b909f67173b4688
Source dataset
uspto-grants-2010_05
Patent number
US07723007B2

Reaction notes

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