HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[3-(4-Ethyl-2,2,7-trimethyl-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-6-yl)-4-trifluoromethoxy-phenyl]-acrylic acid tert-butyl ester → 3-[3-(4-Ethyl-2,2,7-trimethyl-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-6-yl)-4-(2,2,2-trifluoro-ethoxy)-phenyl]-acrylic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[3-(4-Ethyl-2,2,7-trimethyl-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-6-yl)-4-trifluoromethoxy-phenyl]-acrylic acid tert-butyl ester | HCID 68583258 | — |
| Reactant | 3-(4-Ethyl-2,2,7-trimethyl-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-6-yl)-4-(2,2,2-trifluoro-ethoxy)-benzaldehyde | HCID 86611678 | — |
| Product | 3-[3-(4-Ethyl-2,2,7-trimethyl-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-6-yl)-4-(2,2,2-trifluoro-ethoxy)-phenyl]-acrylic acid tert-butyl ester | HCID 68582720 | — |
Reaction Steps
This was made from Compound 2C using a procedure similar to that described for Compound 1E. MS (electrospray): mass calculated for C28H32F3NO5, 519.2; m/z found 520.2, [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723326B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-3a6bd675653e404eb01feffb25355bf1 |
| Source note | uspto-grants-2010_05 |