HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 6-Bromo-2,2,4,7-tetramethyl-4H-benzo[1,4]oxazin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 6-Bromo-4-ethyl-2,2,7-trimethyl-4H-benzo[1,4]oxazin-3-one | HCID 68584741 | — |
| Product | 6-Bromo-2,2,4,7-tetramethyl-4H-benzo[1,4]oxazin-3-one | HCID 68583085 | — |
Reaction Steps
This was prepared using a procedure similar to that described to make Compound 1C, except using methyl iodide in Step 1C. MS (electrospray): mass calculated for C12H14BrNO2, 283.02; m/z found 284 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723326B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-b3955ad1ca7247a99ec72a22352ce633 |
| Source note | uspto-grants-2010_05 |