HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopropane → 6-Bromo-4-isopropyl-2,2,7-trimethyl-4H-benzo[1,4]oxazin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | 6-Bromo-4-ethyl-2,2,7-trimethyl-4H-benzo[1,4]oxazin-3-one | HCID 68584741 | — |
| Product | 6-Bromo-4-isopropyl-2,2,7-trimethyl-4H-benzo[1,4]oxazin-3-one | HCID 68582718 | — |
Reaction Steps
This was prepared using a procedure similar to that described to make Compound 1C, except using l-propyl iodide in Step C. MS (electrospray): mass calculated for C14H18BrNO2, 311.05; m/z found 312 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723326B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-5e7611d6fd2b4fbaa3b001275912b558 |
| Source note | uspto-grants-2010_05 |