HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68574455, compound → HCID 68574581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68574455 | HCID 68574455 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Product | HCID 68574581 | HCID 68574581 | 92% |
Reaction Steps
The title compound was prepared as a white solid in 92% yield (4.10 g) from 1,1-dimethylethyl 6-[(dimethylamino)carbonyl]-2-methyl-4-[(phenylmethyl)oxy]-1H-benzimidazole-1-carboxylate (5.68 g, 13.9 mmol, STEP 1) and 20% palladium hydroxide (2.4 g) by the same manner in STEP 3 of Example 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723321B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-60bc002a718d406f86b7ef342b7a572b |
| Source note | uspto-grants-2010_05 |