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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2239474Generated: October 30, 2026

Dimethylamine → HCID 68408168, compound

https://huagongshe.com/reaction/2239474

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylamineHCID 674—
Reactant4-Bromo-2-(Trifluoromethoxy)Benzene-1-Sulfonyl ChlorideHCID 2736421—
ProductHCID 68408168HCID 6840816881%

Reaction Steps

According to general procedure A, 4-Bromo-2-trifluoromethoxy-benzenesulfonyl chloride (0.35 g, 1.03 mmol) and dimethylamine (10 mL, 33% in ethanol) were stirred in sealed tube for 16 hours. 4-Bromo-N,N-dimethyl-2-trifluoromethoxy-benzenesulfonamide (0.29 g, 81%) was provided after purification. Mp. 55-58° C. MS (ESI) m/z 348.14.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07723332B2
Source datasetuspto-grants-2010_05
ORD IDord-f8929837585e426f9e5eb1a6877ef9f3
Source noteuspto-grants-2010_05