HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Piperidinol, 1-methyl- → HCID 67244148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Piperidinol, 1-methyl- | HCID 66048 | — |
| Reactant | N-((1,1-dimethylethoxy)carbonyl)-beta-alanine | HCID 76809 | — |
| Reactant | HCID 9138898 | HCID 9138898 | — |
| Product | HCID 67244148 | HCID 67244148 | — |
Reaction Steps
The title compound was prepared from 1-methylpiperidin-4-ol and N-(tert-butoxycarbonyl)-β-alanine in a similar manner as described for 2,6-dimethylphenyl 4-[(tert-butoxycarbonyl)amino]butanoate. 1H NMR (400 MHz, CDCl3): δ 4.99 (s, 1H), 4.74-4.79 (m, 1H), 3.32-3.6 (m, 2H), 2.58 (s, 2H), 2.45-2.49 (t, 2H), 2.23 (s, 3H), 2.16-2.19 (m, 2H), 1.83-1.88 (m, 2H), 1.62-1.71 (m, 2H), 1.34 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723333B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-f7c9b748d3c640e5ae32961409e091f0 |
| Source note | uspto-grants-2010_05 |