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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2239607Generated: October 29, 2026

4-Piperidinol, 1-methyl- → HCID 67244148, compound

https://huagongshe.com/reaction/2239607

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Piperidinol, 1-methyl-HCID 66048—
ReactantN-((1,1-dimethylethoxy)carbonyl)-beta-alanineHCID 76809—
ReactantHCID 9138898HCID 9138898—
ProductHCID 67244148HCID 67244148—

Reaction Steps

The title compound was prepared from 1-methylpiperidin-4-ol and N-(tert-butoxycarbonyl)-β-alanine in a similar manner as described for 2,6-dimethylphenyl 4-[(tert-butoxycarbonyl)amino]butanoate. 1H NMR (400 MHz, CDCl3): δ 4.99 (s, 1H), 4.74-4.79 (m, 1H), 3.32-3.6 (m, 2H), 2.58 (s, 2H), 2.45-2.49 (t, 2H), 2.23 (s, 3H), 2.16-2.19 (m, 2H), 1.83-1.88 (m, 2H), 1.62-1.71 (m, 2H), 1.34 (s, 9H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07723333B2
Source datasetuspto-grants-2010_05
ORD IDord-f7c9b748d3c640e5ae32961409e091f0
Source noteuspto-grants-2010_05