Hydrochloric Acid → HCID 86610769, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 2-[3-(naphthalene-1-sulfonylmethyl)-4-nitro-phenyl]-[1,3]dioxolane (3.03 g, 7.6 mmoles), and 2N HCl (4 mL, 8 mmoles) in THF (30 mL) was stirred at 40° C. for 4 hours. The reaction mixture was cooled to room temperature, diluted with waster, extracted with EtOAc, dried over Na2SO4, and concentrated under vacuum to yield the title compound (2.56 g, 7.22 mmoles).

Provenance & Evidence