HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 86610771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 86610772 | HCID 86610772 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86610771 | HCID 86610771 | 100% |
Reaction Steps
1-(3-Chloro-benzyl)-3-(naphthalene-1-sulfonyl)-1H-indazole-5-carbaldehyde (0.18 g, 0.4 mmol) was dissolved in THF and treated under nitrogen with the excess of sodium borohydride (0.2 mmol). After 1 hr the reaction mixture was diluted with water and the product extracted with methylene chloride to afford after evaporation of the solvent the title compound as a colorless solid (0.18 g, 0.4 mmoles).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723329B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-1573997cf5c94fc8acebdf8a889d1c98 |
| Source note | uspto-grants-2010_05 |