HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59305013, compound → HCID 59305021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59305013 | HCID 59305013 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59305021 | HCID 59305021 | — |
Reaction Steps
36 mg of 10% palladium-on-carbon are added to a solution of 170 mg (0.67 mmol) of N-(4-nitrophenyl)-1H-pyrrolo[2,3-b]pyridine-4-amine in 6 ml of ethanol, and the suspension is stirred in a hydrogen atmosphere at atmospheric pressure overnight. The suspension is filtered through Celite and the Celite is washed with ethanol. Concentration under reduced pressure gives the target product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723347B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-9c055d041f9d41b2aa6a6207c3ac8c03 |
| Source note | uspto-grants-2010_05 |