HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 68480823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-[3-(4-chlorophenyl)sulfonyl-2,5-dimethylindol-1-yl]acetic acid | HCID 10407275 | — |
| Reactant | HCID 86605157 | HCID 86605157 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68480823 | HCID 68480823 | — |
Reaction Steps
Sodium hydroxide (1M, 4.3 ml) was added to a solution of the product of example 1 part (c) (1.75 g) in THF (60 ml). The reaction mixture was stirred overnight and then concentrated in vacuo. The residue was recrystallised from water to give the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723373B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-649e2d82c664437ca5b7fcb7cb8878f8 |
| Source note | uspto-grants-2010_05 |