HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 86605158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 68476972 | HCID 68476972 | — |
| Reactant | HCID 86605157 | HCID 86605157 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Product | HCID 86605158 | HCID 86605158 | — |
Reaction Steps
A suspension of the product from example 20 part (c) (1 g) in glacial acetic acid (50 ml) was stirred in the presence of 5% Pt/C (0.5 g) under 3 bar pressure of H2 for 24 hours. The catalyst was removed by filtration and the filtrates concentrated in vacuo. Purification by flash column chromatography (20% EtOAc/hexane as eluent) gave the subtitle compound (0.45 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723373B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-62d30d9c47024f2f973c8c75e89f10ee |
| Source note | uspto-grants-2010_05 |