HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyridine → HCID 11325142, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | HCID 11219135 | HCID 11219135 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 11325142 | HCID 11325142 | 39% |
Reaction Steps
Pyridyl amine was added to organic solvent dissolving 30 mg of 3-(1-benzyl-2-oxo-1,2,5,6-tetrahydro-pyridin-3-yl)-propionic acid (0.12 mM) in EDC. The resulting compound was purified by Silica gel column chromatography with methanol/chloroform (1:20) solvent mixture as an eluant to give 16 mg of the title compound (g1) (yield: 39%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723376B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-b7abfa40421d4202ba8c5182d8c9bc45 |
| Source note | uspto-grants-2010_05 |