1-Bromo-4-chlorobutane → 1-(4-chlorobutyl)-3,4-dihydro-1H-benzo[b]azepine-2,5-dione

Participants

Reaction Steps

Analogously to the procedure described in Example 1, reaction of 3,4-dihydro-1H-1-benzazepine-2,5-dione (11.42 mmol, 2.00 g) and bromo-4-chlorobutane (13.7 mmol, 2.35 g) afforded 1.78 g of the title compound, contaminated with reactants to an extent of 30%. The mixture thus obtained was reacted without further purification.

Provenance & Evidence