N-Hydroxyphthalimide → HCID 59305849, compound

HRID 2240921Notes

Reaction equation

HRID 2240921 reaction equation
[CH:1]([N:4]([CH:8]([CH3:10])[CH3:9])[C:5](Cl)=[S:6])([CH3:3])[CH3:2].[OH:11][N:12]1[C:16](=[O:17])[C:15]2=[CH:18][CH:19]=[CH:20][CH:21]=[C:14]2[C:13]1=[O:22]>>[O:22]=[C:13]1[C:14]2[C:15](=[CH:18][CH:19]=[CH:20][CH:21]=2)[C:16](=[O:17])[N:12]1[O:11][C:5](=[S:6])[N:4]([CH:8]([CH3:10])[CH3:9])[CH:1]([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 15567349HCID 15567349, compound

Product 1

HCID 59305849HCID 59305849, compound

Procedure

This compound was prepared in analogy to example 8 starting from 32.35 g (0.18 mol) of diisopropyl-thiocarbamoyl chloride (prepared as described in (Chem. Ber., 101, (1968), 113) and N-hydroxyphthalimide. Yield 21.44 g of white crystals after recrystallization from hexane, mp. 73-75° C.

Workup

  1. customprepared
  2. customYield 21.44 g of white crystals after recrystallization from hexane, mp. 73-75° C.

Sources & evidence

ORD record
ord-709762b3046a45d89d1d2a292a57f54e
Source dataset
uspto-grants-2010_05
Patent number
US07723399B2

Reaction notes

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