N-Hydroxyphthalimide → HCID 59305850, compound

HRID 2240922Notes

Reaction equation

HRID 2240922 reaction equation
[CH:1]1([N:7]([CH:11]2[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]2)[C:8](Cl)=[S:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[OH:17][N:18]1[C:22](=[O:23])[C:21]2=[CH:24][CH:25]=[CH:26][CH:27]=[C:20]2[C:19]1=[O:28]>>[O:28]=[C:19]1[C:20]2[C:21](=[CH:24][CH:25]=[CH:26][CH:27]=2)[C:22](=[O:23])[N:18]1[O:17][C:8](=[S:9])[N:7]([CH:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1)[CH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 15567350HCID 15567350, compound

Product 1

HCID 59305850HCID 59305850, compound

Procedure

This compound was prepared in analogy to example 8 starting from 24.94 g (0.096 mol) of dicyclohexyl-thiocarbamoyl chloride (prepared as described in (Chem. Ber., 101, (1968), 113) and N-hydroxyphthalimide. Yield 9.65 g of white crystals after recrystallization from hexane, mp. 148-150° C.

Workup

  1. customprepared
  2. customYield 9.65 g of white crystals after recrystallization from hexane, mp. 148-150° C.

Sources & evidence

ORD record
ord-f9a12bf8fa764566b647a333649042b8
Source dataset
uspto-grants-2010_05
Patent number
US07723399B2

Reaction notes

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