HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 25125324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 67538272 | HCID 67538272 | — |
| Reactant | HCID 178485118 | HCID 178485118 | — |
| Product | HCID 25125324 | HCID 25125324 | — |
Reaction Steps
This compound was made in a similar manner to Example 89 Step 8 using 1-(4-(difluoromethoxy)phenyl)-2-m-tolylethane-1,2-dione (1.45 g, 5.0 mmol) from the previous step, 1-methylguanidine hydrochloride (821 mg, 7.5 mmol), Na2CO3 (795 mg, 7.5 mmol), and EtOH (10 mL) to provide 1.04 g, 60%, of the title compound as a beige foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723368B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-7378f13cb24f47d6acdefdbec2328f6b |
| Source note | uspto-grants-2010_05 |