HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 59306504, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 59306469 | HCID 59306469 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59306504 | HCID 59306504 | — |
Reaction Steps
1 mmol of acetic acid 2-[3-cyano-2-((E)-3-phenyl-allanoylamino)-4,7-dihydro-5H-thieno[2,3-c]pyridin-6-yl]-2-oxo-ethyl ester are stirred in 5 ml methanol and 1 ml 45% aqueous NaOH until the reaction is completed. Purification according to the previous preparation affords the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07723523B2 |
| Source dataset | uspto-grants-2010_05 |
| ORD ID | ord-43b386c292e9448694b023e077f3186c |
| Source note | uspto-grants-2010_05 |