関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | 4-Butoxybenzenesulfonyl Chloride | HCID 517990 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-Butoxybenzenesulfonamide | HCID 2049187 | — |
反応手順
100 ml of methanolic ammonia solution were added dropwise to 10 g of 4-n-butoxybenzenesulfonyl chloride, while cooling with ice. After the mixture had been stirred at 20° C. for 1/2 hour, water was added, the mixture was acidified to pH 1 to 2 and the product was filtered off with suction, melting point 99° to 101° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05428046 |
|---|
| 出典データセット | uspto-grants-1995_06 |
|---|
| ORD ID | ord-c44b13c1d4444499a37ed6b544d2882b |
|---|
| 出典メモ | uspto-grants-1995_06 |
|---|
