HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24781111, compound → HCID 59203852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24781111 | HCID 24781111 | — |
| Reactant | HCID 59203840 | HCID 59203840 | — |
| Product | HCID 59203852 | HCID 59203852 | — |
Reaction Steps
The title intermediate was synthesized from tert-butyl [5-(6-methoxy-1,3-benzoxazol-2-yl)pyrimidin-2-yl]carbamate according to the procedure described for tert-butyl (2-fluoroethyl)[5-(6-methoxy-1,3-benzoxazol-2-yl)pyridin-2-yl]carbamate to give 128 mg. 1H NMR 400 MHz, Chloroform-d) δ ppm 9.33 (s, 2H) 7.66 (d, 1H) 7.14 (d, 1H) 7.00 (dd, 1H) 4.79 (t, 1H) 4.67 (t, 1H) 4.42 (t, 1H) 4.37 (t, 1H) 3.90 (s, 3 H) 1.57 (s, 9H) MS m/z 389 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07670591B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-a16b444fab7a4373880947635b28942f |
| Source note | uspto-grants-2010_03 |