HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → 2-Methoxy-6-nitrobenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 2-Methoxy-6-nitrobenzenesulfonyl chloride | HCID 86608853 | — |
| Product | 2-Methoxy-6-nitrobenzenesulfonamide | HCID 66915997 | — |
Reaction Steps
A mixture of 2-methoxy-6-nitro-benzenesulfonyl chloride (12.8 g, 50.87 mmol) and 25% ammonium hydroxide is swirled at 65° C. on a rotavap. After 15 min the volume of the resulting solution is reduced to half by evaporation of volatiles at reduced pressure. Collecting the precipitate by filtration after cooling gives 2-methoxy-6-nitro-benzenesulfonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07671063B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-3504e14a4e6448918d177369d62e6514 |
| Source note | uspto-grants-2010_03 |