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(R)-2-phenylpropionyl chloride → 2-(R)-phenyl-propionic acid (Z)-2-(3,5-dichloro-pyridin-4-yl)-1-(3,4-dimethoxy-phenyl)vinyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (R)-2-phenylpropionyl chloride | HCID 7161075 | — |
| 反応物 | HCID 66881198 | HCID 66881198 | — |
| 生成物 | 2-(R)-phenyl-propionic acid (Z)-2-(3,5-dichloro-pyridin-4-yl)-1-(3,4-dimethoxy-phenyl)vinyl ester | HCID 66899995 | 21% |
反応手順
The compound was obtained starting from 2-(R)-phenyl-propionyl chloride and 2-(3,5-dichloro-pyridin-4-yl)-1-(3,4-dimethoxy-phenyl) -ethanone, following the procedure of Example 7 (0.22 g, 0.48 mmol, 21% yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07671066B2 |
| 出典データセット | uspto-grants-2010_03 |
| ORD ID | ord-841bd23d759b4a869b2c55c4dedca4ef |
| 出典メモ | uspto-grants-2010_03 |