HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → N-[(amino-4-methoxybenzylamino)-methylene]-4-methylbenzene-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 4-Methoxybenzylamine | HCID 75452 | — |
| Reactant | N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide | HCID 178427489 | — |
| Product | N-[(amino-4-methoxybenzylamino)-methylene]-4-methylbenzene-sulfonamide | HCID 67176632 | — |
Reaction Steps
The compound of Example 6 was prepared according to the accompanying synthesis procedure from 0.5 ml of N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide solution (0.2 M, acetonitrile) with 19 mg of methanesulfonic acid and 0.5 ml of 4-methoxybenzylamine solution (1.0 M, acetonitrile) and filed in a substance databank. Calculated mol. wt. 333.41; found mol. wt. (M+H) 334.2; 667.0 (Dimer)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07671074B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-b5ec828d31634012853f5903964b717a |
| Source note | uspto-grants-2010_03 |