Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2242152Generated: October 30, 2026

Methanesulfonic Acid → N-[(amino-4-methoxybenzylamino)-methylene]-4-methylbenzene-sulfonamide

https://huagongshe.com/reaction/2242152

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanesulfonic AcidHCID 6395—
Reactant4-MethoxybenzylamineHCID 75452—
ReactantN-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamideHCID 178427489—
ProductN-[(amino-4-methoxybenzylamino)-methylene]-4-methylbenzene-sulfonamideHCID 67176632—

Reaction Steps

The compound of Example 6 was prepared according to the accompanying synthesis procedure from 0.5 ml of N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide solution (0.2 M, acetonitrile) with 19 mg of methanesulfonic acid and 0.5 ml of 4-methoxybenzylamine solution (1.0 M, acetonitrile) and filed in a substance databank. Calculated mol. wt. 333.41; found mol. wt. (M+H) 334.2; 667.0 (Dimer)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07671074B2
Source datasetuspto-grants-2010_03
ORD IDord-b5ec828d31634012853f5903964b717a
Source noteuspto-grants-2010_03