Methanesulfonic Acid → HCID 178449237, compound

HRID 2242160Notes

Reaction equation

HRID 2242160 reaction equation
C[C:2]1[CH:6]=[C:5]([CH3:7])[N:4]([C:8](=[NH:20])[NH:9][S:10]([C:13]2[CH:18]=[CH:17][C:16]([CH3:19])=[CH:15][CH:14]=2)(=[O:12])=[O:11])N=1.CS(O)(=O)=O.C(N)(CC)C>>[NH2:20][C:8]([NH:4][CH:5]([CH2:6][CH3:2])[CH3:7])=[N:9][S:10]([C:13]1[CH:18]=[CH:17][C:16]([CH3:19])=[CH:15][CH:14]=1)(=[O:11])=[O:12]

Participants

4

Reactant 3

HCID 6395Methanesulfonic AcidHCID 24874Sec-ButylamineHCID 178427489N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide

Product 1

HCID 178449237HCID 178449237, compound

Procedure

The compound of Example 15 was prepared according to the accompanying synthesis procedure from 0.5 ml of N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide solution (0.2 M, acetonitrile) with 19 mg of methanesulfonic acid and 0.5 ml of s-butylamine solution (1.0 M, acetonitrile) and filed in a substance databank. Calculated mol. wt. 269.36; found mol. wt. (M+H) 270.2; 539.1 (Dimer)

Sources & evidence

ORD record
ord-836378037b204cbc9999f874a391d915
Source dataset
uspto-grants-2010_03
Patent number
US07671074B2

Reaction notes

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