Sulfuric Acid → HCID 131727908, compound

HRID 2242376Notes

Reaction equation

HRID 2242376 reaction equation
Cl.[CH3:2][C:3]([CH3:7])=[CH:4][CH2:5][NH2:6].[S:8](=[O:12])(=[O:11])([OH:10])[OH:9]>>[S:8]([O:12][C:3]([CH3:7])([CH2:4][CH2:5][NH2:6])[CH3:2])([OH:11])(=[O:10])=[O:9]

Participants

3

Reactant 2

HCID 1118Sulfuric AcidHCID 183265643-Methylbut-2-en-1-amine hydrochloride

Product 1

HCID 131727908HCID 131727908, compoundYield 85%

Conditions

Temperature
90 °C

Procedure

3-Methyl-2-butene-1-amine hydrochloride (2.86 g, 0.02 mmoles) was dissolved in 5% aqueous sulfuric acid (25 ml) and heated to 90° C. for 18 h. The solvent was removed under reduced pressure yielding 4-amino-2-methyl-butan-2-ol sulfate as a yellow oil (4.73 g, 85%).

Workup

  1. customThe solvent was removed under reduced pressure

Sources & evidence

ORD record
ord-3e882e8534f44a18a1708a5a8f0affbb
Source dataset
uspto-grants-2010_03
Patent number
US07671080B2

Reaction notes

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