Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-Methylbut-2-en-1-amine hydrochloride | HCID 18326564 | — |
| Product | HCID 131727908 | HCID 131727908 | 85% |
Reaction Steps
3-Methyl-2-butene-1-amine hydrochloride (2.86 g, 0.02 mmoles) was dissolved in 5% aqueous sulfuric acid (25 ml) and heated to 90° C. for 18 h. The solvent was removed under reduced pressure yielding 4-amino-2-methyl-butan-2-ol sulfate as a yellow oil (4.73 g, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07671080B2 |
|---|
| Source dataset | uspto-grants-2010_03 |
|---|
| ORD ID | ord-3e882e8534f44a18a1708a5a8f0affbb |
|---|
| Source note | uspto-grants-2010_03 |
|---|
