Trifluoroacetic acid → HCID 57892960, compound

Participants

Reaction Steps

((1S)-1-Azidomethyl-3-methyl-butyl)-carbamic acid tert-butyl ester (9.64 g, 39.78 mmol) was treated with TFA (30 mL) in DCM (150 mL) for 3 hrs, the mixture was evaporated under reduced pressure and the residue was dissolved in ethyl acetate and washed with aqueous 1 M K2CO3, dried with Na2SO4 and concentrated to a yellow liquid (4.55 g, 80%).

Provenance & Evidence