Ammonia → HCID 59204407, compound

Participants

Reaction Steps

Nitrile derivative XXXIV (120 g, 0.43 mol), Raney Ni (30 mL) and ammonia in methanol (750 mL) were placed in a hydrogenator, 15 psi pressure of H2 gas was applied at 60° C. for 12 h. Reaction mass was filtered and the filtrate was concentrated under reduced pressure to give 110 g crude amine XXXV (92%). M+1=282

Provenance & Evidence