HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86618168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 131727927 | HCID 131727927 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86618168 | HCID 86618168 | — |
Reaction Steps
To a solution of the material prepared in Step A (0.017 g, 0.036 mmol) in dichloromethane (3 mL) was added trifluoroacetic acid (1 mL). After 3 h at ambient temperature the reaction was concentrated in vacuo, affording the title compound as a white solid. LC/MS 406.3 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07671073B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-65a7f579667f4414ac3012069349e2da |
| Source note | uspto-grants-2010_03 |