HuagongsheHuagongshe Chemistry Print Report · For research reference only
Maleic Acid → HCID 178465560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Maleic Acid | HCID 444266 | — |
| Reactant | HCID 178465559 | HCID 178465559 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178465560 | HCID 178465560 | — |
Reaction Steps
A 1M solution of maleic acid in acetone (10 ml) is added dropwise to N-(2-phenylbenzothiazol-6-yl)acetamidine (1 g, 0.00374 mol) (Example 1), in acetone (30 ml). The product is precipitated and filtered off. Yield: 1.09 g (77%); Elem. anal. C15H13N3S.C4H4O4; theory C, 59.51; H, 4.47; N, 10.96. found C, 59.30; H, 4.36; N, 10.62. IR (KBr): 3060, 1700, 1480, 1360 cm−1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07674809B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-16884cf5eb024d7eb7308593a19761f2 |
| Source note | uspto-grants-2010_03 |