HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzoic Acid → HCID 4915462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzoic Acid | HCID 9973 | — |
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | 4-Nitro-1,2-phenylenediamine | HCID 5111791 | — |
| Solvent | Toluene ethylacetate | HCID 21584019 | — |
| Product | HCID 4915462 | HCID 4915462 | 76% |
Reaction Steps
Prepared from 4-nitrophenylenediamine and 4-fluorobenzoic acid, in a manner similar to that of Example 9b. Yield: 76%; Rf (7/3 toluene/ethyl acetate): 0.54; IR (KBr): 3312, 1601, 1498, 1333 cm−1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07674809B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-79abb47bae534c988bd4aac37d2abb88 |
| Source note | uspto-grants-2010_03 |