HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzoic acid → HCID 23085767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzoic acid | HCID 11370 | — |
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | 4-Nitro-1,2-phenylenediamine | HCID 5111791 | — |
| Solvent | Toluene ethylacetate | HCID 21584019 | — |
| Product | HCID 23085767 | HCID 23085767 | 76% |
Reaction Steps
Prepared from 4-nitrophenylenediamine and 2-methoxybenzoic acid, in a manner similar to that of Example 9b. Yield: 76%; Rf (6/4 toluene/ethyl acetate): 0.43; IR (KBr): 3005, 1515, 1335, 750 cm−1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07674809B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-effde357019d458bb21acff2e28d5e50 |
| Source note | uspto-grants-2010_03 |