HCID 86600004, compound → HCID 68593512, compound

Participants

Reaction Steps

A mixture of 5% Pd/C (300 mg) and 5-(1-azido-2-ethylbutyl)-1-(4-methoxyphenyl)-1H-pyrazole (882 mg, 2.95 mmol) in methanol (30 mL) was shaken on a Parr apparatus under 3 atm of H2 for 18 h. The reaction was filtered through a plug of Celite, washed well with methanol and concentrated in vacuo to yield the amine in 97% yield as an oil.

Provenance & Evidence