Dimethylformamide dimethyl acetal → HCID 178433912, compound

Participants

Reaction Steps

N,N-Dimethylformamide dimethyl acetal (15 mL) was added to 4-(3-{[4-(3-methyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl)phenyl]thio}phenyl)tetrahydro-2H-pyran-4-carboxamide (2.0 g, 4.88 mmol) (example 10) and the reaction mixture was refluxed for about 2 hours. The solvent was evaporated under reduced pressure to obtain a light brown paste. Yield: 3.0 g.

Provenance & Evidence