HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 4-Amino-3-bromobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4-Aminobenzoic Acid | HCID 978 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-Amino-3-bromobenzoic acid | HCID 238935 | 70% |
Reaction Steps
4-Amino-benzoic acid (100 mmol) was dissolved in DMF (50 mL) and N-bromosuccinimide (100 mmol) was added. Stirred at ambient temperature for 18 h, the reaction mixture was then poured into water (100 mL). The product was removed by filtration, washed with water and dried in vacuo to give 4-amino-3-bromo-benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07674912B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-0bb57b91eb7849a5baba823937559782 |
| Source note | uspto-grants-2010_03 |