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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2243468Generated: November 2, 2026

HCID 68540518, compound → HCID 68546634, compound

https://huagongshe.com/reaction/2243468

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68540518HCID 68540518—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 68546634HCID 68546634100%

Reaction Steps

To a mixture of 4.13 g of the material from Step A and 0.25 g of 10% palladium on carbon was added 150 mL of ethanol. The reaction mixture was stirred under a balloon of hydrogen for three days. The mixture was filtered through celite and the solvent was removed with a rotary evaporator to afford 3.65 g of the title compound as a brown oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07674936B2
Source datasetuspto-grants-2010_03
ORD IDord-b3b5c22300d7433dafd3a0455d2ccfdc
Source noteuspto-grants-2010_03