HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68540518, compound → HCID 68546634, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68540518 | HCID 68540518 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68546634 | HCID 68546634 | 100% |
Reaction Steps
To a mixture of 4.13 g of the material from Step A and 0.25 g of 10% palladium on carbon was added 150 mL of ethanol. The reaction mixture was stirred under a balloon of hydrogen for three days. The mixture was filtered through celite and the solvent was removed with a rotary evaporator to afford 3.65 g of the title compound as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07674936B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-b3b5c22300d7433dafd3a0455d2ccfdc |
| Source note | uspto-grants-2010_03 |