HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58608093, compound → HCID 58608127, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58608093 | HCID 58608093 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 58608127 | HCID 58608127 | — |
Reaction Steps
A mixture of 7-benzyl-3-phenyl-2-(triethylsilanyl)-7H-furo[2,3-b]pyridin-4-one (1) and Pd(OH)2 (0.11 g 20% on C, 0.11 mmol) in ethyl acetate (10 mL) and methanol (10 mL) was degassed and stirred under hydrogen at room temperature for 2.5 hr. The catalyst was filtered off and the solvent was removed to give the title compound. MS (m/z), M+H+ 326.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07674907B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-2302e03a22d6489ba53ed699d12f6149 |
| Source note | uspto-grants-2010_03 |