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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2243590Generated: November 1, 2026

HCID 58608093, compound → HCID 58608127, compound

https://huagongshe.com/reaction/2243590

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58608093HCID 58608093—
CatalystPalladium hydroxideHCID 9942167—
SolventMethanolHCID 887—
SolventEthyl AcetateHCID 8857—
ProductHCID 58608127HCID 58608127—

Reaction Steps

A mixture of 7-benzyl-3-phenyl-2-(triethylsilanyl)-7H-furo[2,3-b]pyridin-4-one (1) and Pd(OH)2 (0.11 g 20% on C, 0.11 mmol) in ethyl acetate (10 mL) and methanol (10 mL) was degassed and stirred under hydrogen at room temperature for 2.5 hr. The catalyst was filtered off and the solvent was removed to give the title compound. MS (m/z), M+H+ 326.0.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07674907B2
Source datasetuspto-grants-2010_03
ORD IDord-2302e03a22d6489ba53ed699d12f6149
Source noteuspto-grants-2010_03