HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 67041439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | HCID 853977 | HCID 853977 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 67041439 | HCID 67041439 | — |
Reaction Steps
A mixture of 8.0 g (0.058 mol) of 1,4,6-trimethylpyrimidin-2(1H)-one and 14.0 g (0.116 mol) of allyl bromide were heated together under reflux in acetonitrile for 16 hours under an inert gas atmosphere. After cooling, a violet solid precipitated out, which was filtered off with suction. The product was purified by recrystallization from chloroform/diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07678156B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-ef11cbd779d548d08125be7732e06cd8 |
| Source note | uspto-grants-2010_03 |