2-Furancarbonyl chloride → HCID 68596857, compound

Participants

Reaction Steps

A mixture of 1,4-Diaza-bicyclo[3.2.2]nonane (0.50 g; 4.0 mmol), 2-furoyl chloride (0.52 mg; 4.0 mmol), diisopropylethylamine (1.02 g; 7.9 mmol) and 1,2-dimethoxyethane (25 ml) was stirred at room-temperatue over night. The product precipitated as hydrochloric acid salt and was filtered and washed with 1,2-dimethoxyethane (5 ml). Yield 0.84 g (82%). Mp. 279-283° C.

Provenance & Evidence