反应详情

The title compound was prepared by stirring a mixture of 5-(4-nitrophenyl)-2-furoic acid (1.0 g; 4.3 mmol) and thionyl chloride (10 ml) at reflux for 2 hours. The mixture was evaporated and co-evaporated with anhydrous toluene. The acid chloride was used without further purification.

1. temperatureat reflux for 2 hours
2. customThe mixture was evaporated
3. customThe acid chloride was used without further purification