HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 5-(4-nitrophenyl)furan-2-carbonyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-(4-Nitrophenyl)-2-furancarboxylic acid | HCID 161593 | — |
| Product | 5-(4-nitrophenyl)furan-2-carbonyl Chloride | HCID 3829983 | — |
Reaction Steps
The title compound was prepared by stirring a mixture of 5-(4-nitrophenyl)-2-furoic acid (1.0 g; 4.3 mmol) and thionyl chloride (10 ml) at reflux for 2 hours. The mixture was evaporated and co-evaporated with anhydrous toluene. The acid chloride was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07678788B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-b7527de1a6af4a3e84b932cb0e0f3ad2 |
| Source note | uspto-grants-2010_03 |