Dichloromethane → HCID 86606176, compound

Participants

Reaction Conditions

Reaction Steps

Ethylisothiocyanate (182 mg; 2.09 mmol) solved in dichloromethane (20 ml) was added dropwise to a mixture of (1,4-diaza-bicyclo[3.2.2]non-4-yl)-5-(4-aminophenyl)-furan-2-yl-methanone and dichloromethane (10 ml) at 5° C. The mixture was allowed to stir for 4 hours at 5° C. and 11 hours at room temperature. The solvent volume was reduced to a third and the solid product was isolated by filtration. Mp. >300° C.

Provenance & Evidence