Hydrazine hydrate (1:1) → HCID 16063625, compound

HRID 2243910Notes

Reaction equation

HRID 2243910 reaction equation
[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[C:3](=O)[C:2]2=O.COP([CH2:16][C:17]([C:19]1[C:20]([C:25]([F:28])([F:27])[F:26])=[N:21][N:22]([CH3:24])[CH:23]=1)=O)(=O)OC.O.[NH2:30][NH2:31]>>[CH3:24][N:22]1[CH:23]=[C:19]([C:17]2[CH:16]=[C:3]3[C:2]([CH:1]4[CH2:7][CH:4]3[CH2:5][CH2:6]4)=[N:31][N:30]=2)[C:20]([C:25]([F:28])([F:27])[F:26])=[N:21]1

Participants

4

Reactant 3

HCID 24654Hydrazine hydrate (1:1)HCID 138696Bicyclo(2.2.1)heptane-2,3-dioneHCID 86609915HCID 86609915, compound

Product 1

HCID 16063625HCID 16063625, compound

Procedure

off-white crystalline solid. MS (EI): 294.2 (M+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, [2-(1-Methyl-3-trifluoromethyl-1H-pyrazol-4-yl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.

Sources & evidence

ORD record
ord-d8f14850d8574b728e2267e3bcb90a42
Source dataset
uspto-grants-2010_03
Patent number
US07678795B2

Reaction notes

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