HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → (1SR,8RS)-5-(5-Chloro-2-trifluoromethyl-phenyl)-3,4-diaza-tricyclo[6.2.1.02,7]undeca-2(7),3,5-triene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Bicyclo(2.2.1)heptane-2,3-dione | HCID 138696 | — |
| Reactant | [2-(5-Chloro-2-trifluoromethyl-phenyl)-2-oxo-ethyl]-phosphonic acid dimethyl ester | HCID 86609919 | — |
| Product | (1SR,8RS)-5-(5-Chloro-2-trifluoromethyl-phenyl)-3,4-diaza-tricyclo[6.2.1.02,7]undeca-2(7),3,5-triene | HCID 16063664 | — |
Reaction Steps
yellow gum. MS (EI): 324.1 (M+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, [2-(5-Chloro-2-trifluoromethyl-phenyl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine mono hydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07678795B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-c257e67ceaab4538995fa6d002175d20 |
| Source note | uspto-grants-2010_03 |