Hydrazine hydrate (1:1) → HCID 16063665, compound

HRID 2243920Notes

Reaction equation

HRID 2243920 reaction equation
[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[C:3](=O)[C:2]2=O.COP([CH2:16][C:17]([C:19]1[CH:24]=[C:23]([F:25])[C:22]([F:26])=[CH:21][C:20]=1[Cl:27])=O)(=O)OC.O.[NH2:29][NH2:30]>>[Cl:27][C:20]1[CH:21]=[C:22]([F:26])[C:23]([F:25])=[CH:24][C:19]=1[C:17]1[N:29]=[N:30][C:2]2[CH:1]3[CH2:7][CH:4]([C:3]=2[CH:16]=1)[CH2:5][CH2:6]3

Participants

4

Reactant 3

HCID 24654Hydrazine hydrate (1:1)HCID 138696Bicyclo(2.2.1)heptane-2,3-dioneHCID 86609918HCID 86609918, compound

Product 1

HCID 16063665HCID 16063665, compound

Procedure

yellow solid. MS (EI): 292.1 (M+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, [2-(2-Chloro-4,5-difluoro-phenyl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.

Sources & evidence

ORD record
ord-21b497724cee4e40a328b65946954875
Source dataset
uspto-grants-2010_03
Patent number
US07678795B2

Reaction notes

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