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Hydrazine hydrate (1:1) → 3-(4-Chloro-2-methyl-phenyl)-5,6,7,8,9,10-hexahydro-cycloocta[c]pyridazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 反応物 | 1,2-Cyclooctanedione | HCID 543698 | — |
| 反応物 | [2-(4-Chloro-2-methyl-phenyl)-2-oxo-ethyl]-phosphonic acid dimethyl ester | HCID 86609922 | — |
| 生成物 | 3-(4-Chloro-2-methyl-phenyl)-5,6,7,8,9,10-hexahydro-cycloocta[c]pyridazine | HCID 16063705 | — |
反応手順
light yellow solid. MS (EI): 286.1 (M+). Prepared from cyclooctane-1,2-dione, [2-(4-Chloro-2-methyl-phenyl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07678795B2 |
| 出典データセット | uspto-grants-2010_03 |
| ORD ID | ord-8effc9dc79624035a95f5823d575b4bc |
| 出典メモ | uspto-grants-2010_03 |