Hydrazine hydrate (1:1) → 3-(4-Chloro-2-methyl-phenyl)-5,6,7,8,9,10-hexahydro-cycloocta[c]pyridazine

HRID 2243931노트

반응식

HRID 2243931 반응식
[C:1]1(=O)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][C:2]1=O.COP([CH2:17][C:18]([C:20]1[CH:25]=[CH:24][C:23]([Cl:26])=[CH:22][C:21]=1[CH3:27])=O)(=O)OC.O.[NH2:29][NH2:30]>>[Cl:26][C:23]1[CH:24]=[CH:25][C:20]([C:18]2[N:30]=[N:29][C:2]3[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:1]=3[CH:17]=2)=[C:21]([CH3:27])[CH:22]=1

참가 물질

4

반응물 3

HCID 24654Hydrazine hydrate (1:1)HCID 5436981,2-CyclooctanedioneHCID 86609922[2-(4-Chloro-2-methyl-phenyl)-2-oxo-ethyl]-phosphonic acid dimethyl ester

생성물 1

HCID 160637053-(4-Chloro-2-methyl-phenyl)-5,6,7,8,9,10-hexahydro-cycloocta[c]pyridazine

실험 절차

light yellow solid. MS (EI): 286.1 (M+). Prepared from cyclooctane-1,2-dione, [2-(4-Chloro-2-methyl-phenyl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.

출처 및 근거

ORD 기록
ord-8effc9dc79624035a95f5823d575b4bc
출처 데이터셋
uspto-grants-2010_03
특허 번호
US07678795B2

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