Hydrazine hydrate (1:1) → HCID 16063742, compound
Reaction equation
[CH3:1][C:2]1([CH3:9])[CH2:6][C:5](=O)[C:4](=O)[CH2:3]1.COP([CH2:16][C:17]([C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=1[Cl:25])=O)(=O)OC.O.[NH2:27][NH2:28]>>[Cl:25][C:20]1[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=1[C:17]1[N:28]=[N:27][C:4]2[CH2:3][C:2]([CH3:9])([CH3:1])[CH2:6][C:5]=2[CH:16]=1Participants
4
Procedure
yellow viscous oil. MS (EI): 258.2 (M+). Prepared from 4,4-dimethyl-cyclopentane-1,2-dione, [2-(2-Chloro-phenyl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.
Sources & evidence
- ORD record
- ord-18f746171ce545e1b75468bc3632a331
- Source dataset
- uspto-grants-2010_03
- Patent number
- US07678795B2
Reaction notes
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