HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → (1SR,8RS)-5-(1-tert-Butyl-5-trifluoromethyl-1H-pyrazol-4-yl)-3,4-diaza-tricyclo[6.2.1.02,7]undeca-2,4,6-triene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Bicyclo(2.2.1)heptane-2,3-dione | HCID 138696 | — |
| Reactant | [2-(1-tert-Butyl-5-trifluoromethyl-1H-pyrazol-4-yl)-2-oxo-ethyl]-phosphonic acid dimethyl ester | HCID 86609927 | — |
| Product | (1SR,8RS)-5-(1-tert-Butyl-5-trifluoromethyl-1H-pyrazol-4-yl)-3,4-diaza-tricyclo[6.2.1.02,7]undeca-2,4,6-triene | HCID 67363888 | — |
Reaction Steps
light yellow crystalline solid. MS (ESI): 336.9 (MH+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, [2-(1-tert-Butyl-5-trifluoromethyl-1H-pyrazol-4-yl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07678795B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-70ecbe4dea444671819addd732f7f159 |
| Source note | uspto-grants-2010_03 |