Hydrazine hydrate (1:1) → HCID 67364681, compound

HRID 2243953Notes

Reaction equation

HRID 2243953 reaction equation
[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[C:3](=O)[C:2]2=O.COP([CH2:16][C:17]([C:19]1[CH:20]=[N:21][N:22]([C:25]([CH3:28])([CH3:27])[CH3:26])[C:23]=1[CH3:24])=O)(=O)OC.O.[NH2:30][NH2:31]>>[C:25]([N:22]1[C:23]([CH3:24])=[C:19]([C:17]2[CH:16]=[C:3]3[C:2]([CH:1]4[CH2:7][CH:4]3[CH2:5][CH2:6]4)=[N:31][N:30]=2)[CH:20]=[N:21]1)([CH3:28])([CH3:27])[CH3:26]

Participants

4

Reactant 3

HCID 24654Hydrazine hydrate (1:1)HCID 138696Bicyclo(2.2.1)heptane-2,3-dioneHCID 86609929HCID 86609929, compound

Product 1

HCID 67364681HCID 67364681, compound

Procedure

light yellow crystalline solid. MS (ESI): 283.2 (MH+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, [2-(1-tert-Butyl-5-methyl-1H-pyrazol-4-yl)-2-oxo-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.

Sources & evidence

ORD record
ord-5bdf6c6f7785454f9a6e3471b36c4a87
Source dataset
uspto-grants-2010_03
Patent number
US07678795B2

Reaction notes

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